High energy milling of Cu2O powders
dc.contributor.author | Dodoo-Arhin, D. | |
dc.contributor.author | Vettori, G. | |
dc.contributor.author | D’Incau, M. | |
dc.contributor.author | Leoni, P. | |
dc.contributor.author | Scardi, P. | |
dc.date.accessioned | 2013-01-03T08:34:38Z | |
dc.date.accessioned | 2017-10-14T06:40:45Z | |
dc.date.available | 2013-01-03T08:34:38Z | |
dc.date.available | 2017-10-14T06:40:45Z | |
dc.date.issued | 2011 | |
dc.description.abstract | X-ray diffraction line profile analysis based on the recently developed Whole Powder Pattern Modelling was used to investigate the microstructure changes in Cu2O powders milled in a vibrating cup mill. The reduction in the average size of coherently scattering domains - and simultaneous narrowing of the size distribution - occurs in the first minutes. An asymptotic limit of ca. 10 nm is obtained. The reduction in size is obtained at the expenses of introducing a massive quantity of dislocations in the system, reaching a limit of ca. 4×10-16 m-2. A proper nanocrystalline microstructure can be obtained for a milling of ca. 20 min. | en_US |
dc.identifier.citation | Z. Kristallogr. Proc. 1 (2011) 75-80 | en_US |
dc.identifier.uri | http://197.255.68.203/handle/123456789/2312 | |
dc.language.iso | en | en_US |
dc.publisher | Oldenbourg Wissenschaftsverlag, München | en_US |
dc.subject | Diffraction | en_US |
dc.subject | High Energy Milling | en_US |
dc.subject | Whole Powder Pattern Modelling | en_US |
dc.title | High energy milling of Cu2O powders | en_US |
dc.type | Article | en_US |